The article discusses the need for high purity welds in industries like pharmaceuticals, semiconductors, and food production due to stringent purity requirements. This has driven the development of specialized purging methods and equipment to prevent oxidation during welding and contamination of the weld. Advances include expanding plugs and inflatable seals to provide gas seals during welding, as well as integrated purge systems that allow for heating and non-destructive testing with the system in place. Monitoring instruments have also been developed to measure low oxygen levels in purge gases. The ASME B31.3 process piping code revisions have further stimulated innovations in purge systems to meet purity standards for applications in these industries.
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Welding Journal ~ Need For Weld Purity Drives Purging Methods
1. PUBLISHED BY THE AMERICAN WELDING SOCIETY TO ADVANCE THE SCIENCE, TECHNOLOGY, AND APPLICATION OF WELDING
AND ALLIED JOINING AND CUTTING PROCESSES WORLDWIDE, INCLUDING BRAZING, SOLDERING, AND THERMAL SPRAYING
July 2012
WELDINGJOURNALVOLUME91NUMBER7JULY2012
July 2012 Cover_4/06 Cover 6/7/12 5:42 PM Page C1
2. 3WELDING JOURNAL
CONTENTS
30 Finishing Stainless Steel Welds for Food Processing
Equipment
Choosing the right finishing abrasives ensures smooth and
corrosion-free welds on food processing equipment
D. Long
36 Need for Weld Purity Drives Purging Methods
The need for high-purity welds in pharmaceuticals, semicon-
ductors, and food production requires purging considerations
M. J. Fletcher
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187-s Scaling Thermocapillary Weld Pool Shape and Transport
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July 2012 Volume 91 Number 7
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On the cover, from top: brazed automotive steel parts (Carmen Paponetti), and
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ponetti); a brazed Portuguese filigree ship model (Michael Y. Reyzer), and torch
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Brazing & Soldering Today
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42 Defect Assessment of Brazed Steel Components
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50 A Composite Solder Alloy Preform for High-Temperature
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60 Managing Precious Metal Volatility in Brazing Alloys
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July 2012_Layout 1 6/7/12 5:20 PM Page 3
3. JULY 201236
Demands for improvements in piping
fabrication quality have risen exponen-
tially in recent years. The latest version
of the ASME 31.3 Process Piping code
(Ref. 1) is a formal recognition of this
emerging requirement that has been
stimulated mainly by the bioprocessing
sector, but also by associated industries
such as pharmaceuticals, semiconduc-
tors, and food production.
An essential element in pipework is
the production of welded joints. The
stringent inspection procedures imposed
by ASME 31.3 apply as much to welded
joints as they do to all the other fabrica-
tion processes involved.
The article noted in Ref. 2 highlighted
more general aspects of the significance
of the latest edition of the code as it ap-
plies to the manufacture of high-quality
pipework. Producers of welding acces-
sories designed specifically to meet the
requirements have been quick to meet
the new challenges ASME B31.3 impose.
The Problem
One of the fundamental requirements
imposed during the welding of pipes is to
prevent oxidation of the weld during the
first pass. The welding torch provides
inert gas coverage of the top of the fu-
sion zone, but unless precautions are
made there is no coverage of the weld
root. The problem has always been rec-
ognized and over the years a variety of
solutions have evolved, some eccentric,
others practical but largely ineffective.
While minimum standards are set for
all fusion welding, the application to the
pharmaceutical, semiconductor, and
food production sectors demands partic-
ularly high standards of cleanliness. Hy-
gienic purity is the driving force for joints
destined for use in pharmaceutical and
food production. Elimination of particu-
late contamination is the crucial require-
ment in semiconductor manufacture.
With some semiconductor manufac-
turers producing chips with dimensions
at the 32-nanometer (nm) level, and re-
search going on at the 15-nm level, it is
easy to see why the design, fabrication,
and maintenance practices required to
ensure exacting purity requirements of
their process fluid distribution systems
are of paramount importance.
In the food processing industries,
statutory legislation and a plethora of lit-
igation suits have forced plant manufac-
turers to introduce quality control levels
previously considered unnecessary. Con-
tamination introduced during fabrication
is now unacceptable.
Need for Weld Purity
Drives Purging Methods
MICHAEL J. FLETCHER
(barrow@post.com) is chief
executive officer, Delta
Consultants, Rutland, UK.
BY MICHAEL J. FLETCHERDesign, fabrication, and maintenance practices that
can meet exacting purity requirements of ASME 31.3
are crucial to the food, pharmaceutical, and
semiconductor industries
Fig. 1 Schematic section through tube joint illustrating gas seals on each side of the weld.
The identifiers show access routes for inert gas supply/exhaust.
Fig. 2 Nylon/rubber expanding plug in
common use for tube sealing.
Fig. 3 Inflatable neoprene pipe seal.
Fletcher Feature July 2012_Layout 1 6/6/12 8:07 AM Page 36
4. The Solution
Satisfying the high level of protection
lies in selection of specialized purging
equipment. Inserting low-quality paper
or other barrier material on either side
of the joint and filling the space between
them with inert gas may be good enough
for low-level requirements but is unsuit-
able to meet the requirements ASME
B31.3 imposes.
Significant progress was made in
purging equipment in the 1980s when
welding accessory manufacturers devel-
oped expanding plugs and inflatable
stoppers (Figs. 13). These devices gave
assurance of effective sealing with the
pipe wall and prevented leakage of inert
gas from the weld zone, thus precluding
backflow of oxidizing gases from the at-
mosphere.
Generally effective, these develop-
ments still allowed considerable scope
for innovative improvements. Devices
such as shown in Fig. 4 integrate a pair
of inflatable bladders and provides pres-
sure-controlled gas ports for both inflat-
ing and inert gas supplies.
Other systems have been designed to
satisfy the requirements of pre- and post-
weld heating through the use of thermally
resistant materials Fig. 5. Some are
produced with no metallic materials in
the weld vicinity so that postweld nonde-
structive examination can be undertaken
with the purge system still in place.
There have been significant develop-
ments recently in gas-monitoring instru-
ments. These incude devices such as
monitors (Fig. 6) designed specifically
for measurement of low oxygen levels in
purge gases during welding.
The challenges of the ASME Process
Piping code have provided a stimulus for
further developments, and advanced ver-
sions of commercial purge systems are
becoming available. Some of these em-
ploy high-stability engineering polymers
to cover all exposed metal components
so that the risk of transfer of metallic ma-
terials onto pipe surfaces is minimized.
Many are able to provide fully automatic
control over inert gas flow and pressure.
The welding supply industry is re-
sponding proactively to the demands
imposed by the latest edition of ASME
31.3.
References
1. ASME B31.3, Process Piping, Chap-
ter X, High Purity Piping. 2010. New
York, N.Y.: American Society of Me-
chanical Engineers.
2. Huitt, W. M., Henon, B. K., and
Molina III, V. B. 2011. New piping code
for high-purity processes. Chemical En-
gineering, July.
37WELDING JOURNAL
Fig. 4 This purge system was designed
specifically for rapid deployment and in足
corporates gas entry and exit routes.
Fig. 5 Thermally tolerant, fully inte足
grated purge systems developed for use
where pre足 and postweld heating is re足
quired
Fig. 6 Sensitive monitoring instrument
for measuring oxygen content in purge
gas.
4
6
5
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Fletcher Feature July 2012_Layout 1 6/6/12 8:08 AM Page 37