際際滷

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Akademia im. Jana Dugosza w
                       Czstochowie
    Wydzia: Matematyczno-Przyrodniczy

    Kierunek: Ochrona rodowiska
    Specjalno: Analiza rodowiskowa



KARBONIZATY Z ZIAREN ZB纏 
  BUDOWA I WACIWOCI

                                 Agnieszka Kurczakowska

                                              Promotor:
                              dr hab. Wojciech Ciesielski
                             Katedra Chemii Organicznej
Cel pracy


Przedstawienie bada dotyczcych wykorzystania
ziaren zb坦甜 r坦甜nego pochodzenia botanicznego
(jczmienia, owsa, pszenicy, pszen甜yta, 甜yta) jako
添r坦da biopaliw poprzez degradacj do gazu
syntezowego i karbonizatu.
Przeprowadzona praca opieraa si na badaniach:

 analizy termicznej (DSC) oraz termograwimetrycznej
  (TG/DTG) w celu sprawdzenia procesu termicznego
  rozkadu ziarna,
 analizy chemicznej w mikroobszarach (EDS) w celu
  zapoznania si ze skadem pierwiastkowym
  powierzchni ziarna,
 skaningowej mikroskopii elektronowej (SEM) w celu
  obserwacji r坦甜nych typ坦w ziaren zb坦甜 i ich
  por坦wnania.
Przebieg degradacji ziaren z wydzieleniem CO i CO 2
jest najlepszy dla jczmienia i pszen甜yta.
Ilo powstaego karbonizatu jest niska.




     Analiza termiczna (DSC) i termograwimetryczna (TG, DTG)
              dla ziarna jczmienia i ziarna pszen甜yta
Najlepszymi zbo甜ami w celu uzyskania znacznej iloci
karbonizatu s ziarna owsa i油pszenicy.




        Analiza termiczna (DSC) i termograwimetryczna (TG, DTG)
                    dla ziarna owsa i ziarna pszenicy
Skaningowa mikroskopia elektronowa (SEM)




       Karbonizaty ziarna jczmienia i ziarna owsa
Skaningowa mikroskopia elektronowa (SEM)




Karbonizaty ziarna pszenicy, ziarna pszen甜yta i ziarna 甜yta
Analiza skadu pierwiastkowego powierzchni ziaren
                 wykonana metod
 analizy chemicznej w mikroobszarach (EDS)




         Analiza chemiczna w mikroobszarach (EDS)
            dla ziarna jczmienia i ziarna 甜yta.
Wnioski
   Badania termiczne pokazuj, i甜 w odpowiedni spos坦b mo甜na
    sterowa procesami termolizy tak aby uzyska po甜dane iloci
    albo karbonizatu albo produkt坦w lotnych.


   Ziarna zb坦甜 (tak甜e z teren坦w ska甜onych) mo甜na najwydajniej
    wykorzysta do produkcji biopaliw przez zgazowanie badanej
    biomasy.
Wnioski
   Badania termiczne pokazuj, i甜 w odpowiedni spos坦b mo甜na
    sterowa procesami termolizy tak aby uzyska po甜dane iloci
    albo karbonizatu albo produkt坦w lotnych.

   Ziarna zb坦甜 (tak甜e z teren坦w ska甜onych) mo甜na najwydajniej
    wykorzysta do produkcji biopaliw przez zgazowanie badanej
    biomasy.

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Prezentacja pracy mgr a.kurczakowska

  • 1. Akademia im. Jana Dugosza w Czstochowie Wydzia: Matematyczno-Przyrodniczy Kierunek: Ochrona rodowiska Specjalno: Analiza rodowiskowa KARBONIZATY Z ZIAREN ZB纏 BUDOWA I WACIWOCI Agnieszka Kurczakowska Promotor: dr hab. Wojciech Ciesielski Katedra Chemii Organicznej
  • 2. Cel pracy Przedstawienie bada dotyczcych wykorzystania ziaren zb坦甜 r坦甜nego pochodzenia botanicznego (jczmienia, owsa, pszenicy, pszen甜yta, 甜yta) jako 添r坦da biopaliw poprzez degradacj do gazu syntezowego i karbonizatu.
  • 3. Przeprowadzona praca opieraa si na badaniach: analizy termicznej (DSC) oraz termograwimetrycznej (TG/DTG) w celu sprawdzenia procesu termicznego rozkadu ziarna, analizy chemicznej w mikroobszarach (EDS) w celu zapoznania si ze skadem pierwiastkowym powierzchni ziarna, skaningowej mikroskopii elektronowej (SEM) w celu obserwacji r坦甜nych typ坦w ziaren zb坦甜 i ich por坦wnania.
  • 4. Przebieg degradacji ziaren z wydzieleniem CO i CO 2 jest najlepszy dla jczmienia i pszen甜yta. Ilo powstaego karbonizatu jest niska. Analiza termiczna (DSC) i termograwimetryczna (TG, DTG) dla ziarna jczmienia i ziarna pszen甜yta
  • 5. Najlepszymi zbo甜ami w celu uzyskania znacznej iloci karbonizatu s ziarna owsa i油pszenicy. Analiza termiczna (DSC) i termograwimetryczna (TG, DTG) dla ziarna owsa i ziarna pszenicy
  • 6. Skaningowa mikroskopia elektronowa (SEM) Karbonizaty ziarna jczmienia i ziarna owsa
  • 7. Skaningowa mikroskopia elektronowa (SEM) Karbonizaty ziarna pszenicy, ziarna pszen甜yta i ziarna 甜yta
  • 8. Analiza skadu pierwiastkowego powierzchni ziaren wykonana metod analizy chemicznej w mikroobszarach (EDS) Analiza chemiczna w mikroobszarach (EDS) dla ziarna jczmienia i ziarna 甜yta.
  • 9. Wnioski Badania termiczne pokazuj, i甜 w odpowiedni spos坦b mo甜na sterowa procesami termolizy tak aby uzyska po甜dane iloci albo karbonizatu albo produkt坦w lotnych. Ziarna zb坦甜 (tak甜e z teren坦w ska甜onych) mo甜na najwydajniej wykorzysta do produkcji biopaliw przez zgazowanie badanej biomasy.
  • 10. Wnioski Badania termiczne pokazuj, i甜 w odpowiedni spos坦b mo甜na sterowa procesami termolizy tak aby uzyska po甜dane iloci albo karbonizatu albo produkt坦w lotnych. Ziarna zb坦甜 (tak甜e z teren坦w ska甜onych) mo甜na najwydajniej wykorzysta do produkcji biopaliw przez zgazowanie badanej biomasy.