Nucleair magnetic resonance
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Nucleair magnetic resonance
- 1. Nucleair Magnetic Resonance Door: Patrick van Dorst
- 2. Inhoud Geschiedenis Mijn werkzaamheden Resultaat verwerking
- 3. Geschiedenis Piet Gorbet 19 september 1938
- 5. De werkzaamheden Algemene werkbeschrijving Aanvragen van LIMS-nummers
- 6. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg)
- 7. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3
- 8. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3 NMR-buisjes nummeren
- 9. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3 NMR-buisjes nummeren Gegevens verwerking in het Automation System van de NMR auto sampler
- 10. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3 NMR-buisjes nummeren Gegevens verwerking in het Automation System van de NMR auto sampler NMR-buisjes voorzien van het samplevloeistof
- 11. De werkzaamheden Algemene werkbeschrijving : Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3 NMR-buisjes nummeren Gegevens verwerking in het Automation System van de NMR auto sampler NMR-buisjes voorzien van het samplevloeistof NMR-buisjes in de autosampler zetten
- 12. De werkzaamheden Algemene werkbeschrijving: Aanvragen van LIMS-nummers Afwegen van de samples (70mg) Samples oplossen in 1 ml CDCl3 NMR-buisjes nummeren Gegevens verwerking in het Automation System van de NMR auto sampler NMR-buisjes voorzien van het samplevloeistof NMR-buisjes in de autosampler zetten Automation starten
- 14. Resultaat verwerking Wat moet er bepaald worden? De compositie Monomeer 1 Monomeer 2 BPA (Bisphenolaceton) De (standaard) eindgroepen OH-eindgroepen Zegt iets over de conversie van de reactie Bijproducten/nevenreacties/degradatieproducten 5 verschillende Negatief effect op eigenschappen van het polymeer Proberen te minimaliseren
- 15. Resultaat verwerking NetNMR Intergreren van pieken Monomeer 1 Monomeer 2 BPA (Bisphenolaceton\ Eindgroepen Bijproducten
- 16. Resultaat verwerking monomeer 2 monomeer 1 monomeer 1 bijproduct 1 bijproduct 2 Eindgroep bijproduct 3
- 17. Resultaat verwerking NetNMR Intergreren Excel Component Analysis
- 18. Resultaat verwerking Microsoft excel Component Analysis Tabel Concentratie van de componenten Omrekenen van Bijproduct 2 (Mol%) (PPM) #(PPM)= 12617 0.01 2212 1.65 1.42 1.68 6.9 14.8 73.5 887 f5 12611 0.01 2108 1.57 1.47 1.74 6.9 14.9 73.5 887 f4 12192 0.01 2263 1.68 1.64 1.84 6.8 14.7 73.3 887 f1 24427 0.00 536 0.42 1.15 1.03 7.7 13.1 76.5 887 s8 24931 0.02 435 0.34 0.97 0.84 7.8 13.5 76.6 887 s6 27338 0.00 255 0.20 1.04 0.97 7.9 13.5 76.4 887 s1 Mw Bijproduct 3 (mol%) Bijproduct 2 (PPM) Bijproduct 2 (mol%) Bijproduct 1 (mol%) Eindgroep (mol%) Monomeer 2 (mol%) BPA (mol%) Monomeer 1 (mol%) Run nummer
- 19. Conclusie S-samples Minder vrij Msc Monomeer 1 < acceptabel Eindproduct F-samples Meer vrij MsC Monomeer 1 < onacceptabel Tussentijds 6,9 mol% 7,8 mol% 7 mol% Monomeer 2 14,8 mol% 13,4 mol% 13 mol% BPA 73,4 mol% 76,5 mol% 80 mol% Monomeer 1 Aanwezig in F-samples Aanwezig in S-samples Theoretisch Stof
- 20. Conclusie MSC MSC F-sample S-sample
- 21. Bedankt voor jullie aandacht Zijn er nog vragen?